Nanjing Y Bio-pharmaceutical Inc. Address: Building B, Dingyebaitai Mansion 10 Xinhuo Road Gaoxin DistrictNanjing city, Jingsu Province China Zip code: 210032 Tel:86-25-58855549 Fax: 86-25-58855691 email: lygydd@ 检 验 报 告 书 REPORT FOR TESTING QUALITY 品名:Boc-L-叔亮氨酸 PRODUCT:Boc-L-tert-Leucine CAS:62965-35-9 Batch No. 2016020302 Mfg. DATE 2016-02-03 Packing 25 kg/Drum Expiry Date 2018-02-06 Quantity 500kg Report Date 2016-02-15 Standard Enterpise Standard SI. No. Test parameter Specification Result 1 Appearance white to off-white powder White powder 2 Identification IR and HPLC Conforms 3 Water content by KF (% w/w) ≤0.5% 0.04% 4 Loss on drying ≤1.0% 0.25% 5 Residue on ignition (% w/w) ≤0.2% 0.10% 6 Enantiomer content by chiral HPLC ≤0.1% Not detected 7 Purity by HPLC ≥98.0% 99.15% a. N-Acetyl L-tertiary Leucine ≤0.05% Not detected b. Methoxycarbonyl -L-Valine ≤0.10% Not detected c. Any individual unknown impurity ≤0.3% 0.20% d. Total impurities ≤1.0% 0.20% 8 Assay by Titration 98.0% to 102.0% 100.24%